Metal-Free Decarboxylative Three Component Coupling.
Phenylpropiolic acid synthesis essay; 2012 essay competitions for college; College essay sample significant personal accomplishments; Product design and process analysis essay.
In this exercise, the goal was to produce acetylsalicylic acid through the organic synthesis from the reaction of salicylic acid to acetic anhydride, the starting materials. Instead of using acetic acid, acetic anhydride was used as solvent since the anhydride reacting with water to form acetic acid tends to drive the reaction to the right.
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The conversion of phenylpropiolic acid to the anhydride of 1phenylnaphthalene-2,3,-dicarboxylic acid by the action of acetic anhydride was first observed by Michael and Bucher. 4 The early history of this reaction has been reviewed5 and the generality demonstrated. 6 In particular, Haworth and Kelly? reported that piperonplpropiolic acid(IV), on heating under reflux with acetic anhydride.
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Acetic acid of phenylpropiolic acid (PhPA) is an effective terminator, so PhPA can not be directly polymerized. After adding NaOH, the monomer is conversion into sodium salt.
Structure, properties, spectra, suppliers and links for: phenylpropiolic acid, 637-44-5.